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Liquid waveguide spectrophotometric measurements of arsenate and particulate arsenic, as well as phosphate and particulate phosphorus, in seawater
https://oacis.repo.nii.ac.jp/records/1723
https://oacis.repo.nii.ac.jp/records/17237e660931-604f-4e7e-a899-be1f553f8153
名前 / ファイル | ライセンス | アクション |
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15H02802_JO_73-4-439 (330.7 kB)
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Item type | 学術雑誌論文 / Journal Article(1) | |||||
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公開日 | 2019-04-22 | |||||
タイトル | ||||||
タイトル | Liquid waveguide spectrophotometric measurements of arsenate and particulate arsenic, as well as phosphate and particulate phosphorus, in seawater | |||||
言語 | ||||||
言語 | eng | |||||
キーワード | ||||||
主題 | Arsenate, Phosphate, Particulate arsenic, Particulate phosphorus, Liquid waveguide spectrophotometry | |||||
資源タイプ | ||||||
資源タイプ | journal article | |||||
著者 |
Hashihama, Fuminori
× Hashihama, Fuminori× Suwa, Shuhei× Kanda, Jota |
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書誌情報 |
Journal of Oceanography 巻 73, 号 4, p. 439-447, 発行日 2017-08 |
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抄録 | ||||||
内容記述 | Sensitive methods for the determination of arsenate and particulate arsenic (PAs), as well as phosphate and particulate phosphorus (PP), in seawater are described. The method for arsenate and phosphate was established by applying automated liquid waveguide spectrophotometry. Because the reaction time for the formation of arsenate-molybdate complex is longer than that for phosphate-molybdate complex, a long Teflon tube submerged in a heating bath was installed in the conventional phosphate flow system. The arsenate was quantified as the difference between absorbances of molybdenum blue dyes with (only phosphate) and without (phosphate + arsenate) arsenate reduction treatment. Contamination was observed in the reagent for arsenate reduction and must be corrected. Linear dynamic ranges up to 1000 nM were confirmed for arsenate and phosphate. The detection limits for arsenate and phosphate were 5 and 4 nM, respectively. Freezing was a reliable sample preservation technique for both arsenate and phosphate. The method for PAs and PP was established by combining conventional persulfate oxidation of PP and the automated liquid waveguide spectrophotometry of arsenate and phosphate. The digestion efficiencies of organic As analogs were >93%. Contamination in the glass fiber filter was negligible. Field tests confirmed that the coefficients of variation (CVs) of 10–19 nM arsenate and 4–151 nM phosphate were 7–20% and 1–25%, respectively, while the CVs of 0.9 nM PAs and 10.2 nM PP were 11 % and 4 %, respectively. | |||||
ISSN | ||||||
収録物識別子タイプ | ISSN | |||||
収録物識別子 | 09168370 | |||||
書誌レコードID | ||||||
収録物識別子タイプ | NCID | |||||
収録物識別子 | AA10833529 | |||||
DOI | ||||||
関連タイプ | isVersionOf | |||||
識別子タイプ | DOI | |||||
関連識別子 | https://doi.org/10.1007/s10872-017-0412-6 | |||||
権利 | ||||||
権利情報 | (c) 2017 The Oceanographic Society of Japan and Springer Japan. This is the author's version of the work. It is posted here for your personal use. Not for redistribution. The definitive Version of Record was published in https://doi.org/10.1007/s10872-017-0412-6 | |||||
情報源 | ||||||
関連識別子 | https://doi.org/10.1007/s10872-017-0412-6 | |||||
関連名称 | Publisher's Version/PDF | |||||
情報源 | ||||||
関連識別子 | http://kaiyo-gakkai.jp/jos/ | |||||
関連名称 | 日本海洋学会 | |||||
情報源 | ||||||
関連識別子 | https://kaken.nii.ac.jp/ja/grant/KAKENHI-PROJECT-15H02802/ | |||||
関連名称 | KAKEN研究課題: 天然放射性リン同位体による亜熱帯海域のリン供給過程の解明 | |||||
情報源 | ||||||
関連識別子 | https://nrid.nii.ac.jp/ja/nrid/1000060202032/ | |||||
関連名称 | 研究代表者: 神田穣太 (東京海洋大学) | |||||
著者版フラグ | ||||||
出版タイプ | AM | |||||
出版タイプResource | http://purl.org/coar/version/c_ab4af688f83e57aa | |||||
件名 | ||||||
主題 | 科学研究費研究成果 | |||||
論文ID(NAID) | ||||||
関連タイプ | isVersionOf | |||||
識別子タイプ | NAID | |||||
関連識別子 | 40021269042 | |||||
出版者 | ||||||
出版者 | Springer Japan | |||||
科学研究費研究課題 | ||||||
主題 | 天然放射性リン同位体による亜熱帯海域のリン供給過程の解明 | |||||
科学研究費研究課題 | ||||||
主題 | Cosmogenic radiotracer study of phosphorus cycling in oligotrophic subtropical ocean | |||||
研究課題番号 | ||||||
内容記述 | 15H02802 |